Typical G.C. analysis

硼化镁 boronia megastigma nees absolute
#%LeftshiftComponents
380.102-acetoxylinalool A + 十三烷 tridecane + methyl 2-methoxybenzoate
580.02 acetvanillone + (E)-beta-farnesene
320.45(E)-茴香脑 anethole + 藏红花 safrol + nonanoic acid
87trace 蜂胶 apiole
48.015 benzyl 3-丁酸甲酯 methyl butyrate + (Z)-retro-gamma-ionone
40.01  苯甲醇 benzyl alcohol
970.06  苯甲酸苄酯 benzyl benzoate
880.20beta-bisabolol + tetradecanol
340.10异 isobornyl acetate + menthyl acetate
400.02trans-carvyl acetate + (E)-linalool
540.04beta- 石竹烯 caryophyllene
730.09  石竹烯氧化物 caryophyllene oxide
120.01  菊花酮 chrysanthenone
651.20sesqui 桉树脑 cineole
86trace  coniferyl methyl ether
410.07 cyclic beta-ionone
470.03 decanoic acid + 2-甲基丁酸苄酯 benzyl 2-methyl butyrate + (Z)-retro-gamma-ionone
220.012- decanol
310.06 decanol + 5-hydroxylinalool B + methyl 2-isobutyr氧 oxy-3-methyl valerate
210.602-decanone + 7-hydroxy丁烯醇 hotrienol
570.657,8-二氢β-紫罗兰醇 dihydro-beta-ionol + (Z)-retro-alpha-ionone
551.307,8- 二氢β-紫罗兰酮 dihydro-beta-ionone
630.06 dihydroactinodiolide + undecyl acetate
230.01 十二烷 dodecane + 紫丁香 lilac alcohol
500.042- dodecanol
763.80 dodecyl acetate + 8-hydroxy芳樟基 linalyl isobutyrate
108trace  二十烷 eicosane
420.01delta- elemene
700.097,11-epoxymegastigm-5(6)-en-9-one
490.01  癸酸乙酯 ethyl decanoate
950.08(E,E)- 法尼醇 farnesol
28trace  香叶醇 geraniol
460.70 乙酸香叶酯 geranyl acetate + 香兰素 vanillin
56trace  香叶基丙酮 geranyl acetone
1114.30(E)-4-(香叶基 geranyl oxy) 肉桂酸 cinnamic acid
1061.90(Z)-4-(香叶基 geranyl oxy) 肉桂酸 cinnamic acid
90.02  guaiacol
940.70  heptadecane
770.04  十hexadecane
590.03alpha- humulene
750.03  humulene oxide I
850.303- hydroxy-beta-ionone
430.208- hydroxylinalool
910.108-hydroxy芳樟基 linalyl 2-丁酸甲酯 methyl butyrate
1132.208-hydroxy芳樟基 linalyl decanoate
1160.308-hydroxy芳樟基 linalyl 十二酸酯 dodecanoate
1050.308-hydroxy芳樟基 linalyl heptanoate
1091.808-hydroxy芳樟基 linalyl heptanoate
920.108-hydroxy芳樟基 linalyl isovalerate
1120.708-hydroxy芳樟基 linalyl nonanoate
690.208-hydroxy芳樟基 linalyl propionate
990.308-hydroxy芳樟基 linalyl tiglate
1181.408-hydroxy芳樟基 linalyl 十三酸酯 tridecanoate
980.098-hydroxy芳樟基 linalyl valerate
802.40(E)-3-hydroxymegastigm-7-en-9-one
680.03(z)-3 Z)-3-hydroxymegastigm-7-en-9-one
1070.09N-(2-(4-hydroxyphenyl)ethyl) 2-methyl butyramide
1100.20N-(2-(4-hydroxyphenyl)ethyl) tiglamide
1159.30N-(2-(4-hydroxyphenyl)ethyl) tiglamide + methyl (Z)-4-(香叶基 geranyl oxy) cinnamate
840.154-oxo-beta- 紫罗兰 ionol
520.30beta-紫罗兰 ionol + 4,5-epoxy-gamma-homo环cyclocitral
710.64(E,E)-pseudo- ionone
450.05(Z)-alpha-ionone + (Z)-carvyl -carvyl acetate
530.04(E)-alpha-ionone + 2,6-dimethyl-4-methyl phenol
6114.90(E)-beta-ionone + alpha-curcumene + 5,6-epoxy-beta-ionone
670.02  斜烷醚 italicene ether
820.35delta-jasmonic acid lactone (syn) + 4-hydroxy-beta-ionone
890.70delta-jasmonic acid lactone )反 anti) + methyl curcubate
50.45  柠檬烯 limonene
290.20 芳樟基 linalyl acetate + 5-hydroxylinalool A
740.30(E)-megastigm-7-en-3,9-二酮 9-dione
140.15para-mentha-1,3,8-triene +camphor
30.06para- mentha-1,5,8-triene
1176.70 methyl (E)-4-(香叶基 geranyl oxy) cinnamate
960.50  methyl (E)-4-hydroxycinnamate
830.70  (z)-表茉莉酸甲酯 methyl (Z)-epi-jasmonate
791.20 (z)-茉莉酸甲酯 methyl (Z)-jasmonate + (E)-3-hydroxymegastigm-7-en-9-one
10.10 methyl 1-hydroxy-3-methyl valerate + beta-松油萜、蒎烯 pinene
440.20 methyl 2-(2-methyl butyoxy)-3-methyl valerate + neryl acetate
150.06 methyl 2-acetoxy-3-methyl valerate
810.70 methyl 2,3-di-epi-curcubate + 4-oxo-beta-ionone
9014.60 methyl 3-epi-curcubate + (Z)-8-heptadecene
18tracepara- 甲基苯乙酮 methyl acetophenone
240.01  壬酸甲酯 methyl nonanoate
130.01  辛酸甲酯 methyl octanoate
1040.02  棕榈酸甲酯 methyl palmitate
20.40 myrcene + octanal
250.20 橙花醇 nerol + (E)-tagetenone
1030.08  十八烷 nonadecane
100.75 nonanal + linalool + 丁烯醇 hotrienol + 2-苯乙醇 phenethyl alcohol
19trace  nonanol
110.082- nonanol
70.07(E)-beta- 罗勒烯 ocimene
60.02(Z)-beta- 罗勒烯 ocimene
1010.03  十八烷 nonadecane
200.07  octanoic acid
80.03  辛基酚聚醚 octanol
640.16 十五烷 pentadecane + iso斜烷醚 italicene ether
102trace  乙酸十五烷基酯 pentadecyl acetate
620.05endoperoxide of cyclic beta-ionone
660.02beta-sesqui 芹菜烯 phellandrene
30trace异 isopiperitenone + geranial
270.01  piperitone
720.55 芦丁烯醇 spathulenol + (E)-9-hydroxymegastigm-7-en-3-one
780.09 syringl methyl ether + 姜油酮 zingerone
260.30(Z)-tagetenone + 茴香醛 anisaldehyde
160.02(E)- 戊烯酮 tagetone
170.03(Z)- 戊烯酮 tagetone
35trace  terpinen-4-yl acetate
510.02  tetradecane
1000.50  乙酸十四烷基酯 tetradecyl acetate
370.03 theaspirane A + 2-undecanol
392.40 theaspirane A + 2-acetoxylinalool B + m癸酸乙酯 ethyl decanoate
1140.03  十三烷 tricosane
930.15  乙酸十三烷基酯 tridecyl acetate
360.05  十一醛 undecanal
601.00 undecanoic acid + 8-hydroxyl 芳樟基 linalyl acetate + dodecanol + 2-异戊酸苯乙酯 phenethyl isovalerate + tigtig苄基酯 benzyl tiglate
330.052-十一烷酮 undecanone + bornyl acetate

P. Weyerstahl, H. 马绍尔 Marschall, W-R. bork Bork, R. r Rilk, S. 施耐德 Schneider h-c h H-C. Wahlburg, 成分 Constituents of the 精华/精粹/精萃 absolute of boronia Boronia megastigma 内斯 Nees from 塔斯马尼亚 Tasmania. Flav. Fragr. J., 10, 297-311 (1995).

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michelia champaca champaca浸膏
#%LeftshiftComponents
520.05异 iso 苯甲酸戊酯 amyl benzoate
360.035-戊基 amyl-3,4-dimethyl 异恶唑 isoxazole
370.023-戊基 amyl-4,5-dimethyl 异恶唑 isoxazole
244trace(E)- 茴香脑 anethole
1400.03  benzaldehyde
730.10(E+Z)- 苯甲醛肟 benzaldoxime
1590.20  benzoic acid
2160.01 benzyl (z)-3 Z)-3-hexenoate
212trace  2-甲基丁酸苄酯 benzyl 2-methyl butyrate
250.60  乙酸苄酯 benzyl acetate
382.00  苯甲醇 benzyl alcohol
901.00  苯甲酸苄酯 benzyl benzoate
211trace  丁酸苄酯 benzyl butyrate
210.10  甲酸苄酯 benzyl formate
2130.03  异戊酸苄酯 benzyl isovalerate
240trace  苄基甲基醚 benzyl methyl ether
2170.20  乙酸苄基苯酯 benzyl phenyl acetate
2180.10 benzyl phenyl propionate
209trace  丙酸苄酯 benzyl propionate
2150.02  tigtig苄基酯 benzyl tiglate
2140.04  戊酸苄酯 benzyl valerate
1220.10  borneol
2030.03  bornyl acetate
1680.01  博伏利特 bovolide
210trace  苯甲酸丁酯 butyl benzoate
1010.03beta- 石竹烯 caryophyllene
640.20  石竹烯氧化物 caryophyllene oxide
40.031,8- 桉树脑 cineole
750.30  肉桂醇 cinnamic alcohol
1430.02  肉桂醛 cinnamic aldehyde
2510.01  肉桂醛 cinnamic aldehyde 肟 oxime
256trace  肉桂腈 cinnamonitrile
710.10(E)- 醋酸肉桂酯 cinnamyl acetate
2310.05  肉桂酸苯甲酸酯 cinnamyl benzoate
2280.01  肉桂酸甲酸酯 cinnamyl formate
2290.01  肉桂酸cinnamyl isovalerate
2300.05  肉桂酸cinnamyl tiglate
1720.01  香豆素 coumarin
1340.02  甲酚 creosol
133tracepara- 甲酚 creosol
570.04  cubenol
530.02epi- cubenol
139tracebeta- 环cyclocitral
169trace  decan-5-olide
1180.05  decanol
170trace(Z)-7- decen-5-olide
1540.10  脱氢β-紫罗兰酮 dehydro-beta-ionone
155trace 脱氢β-紫罗兰酮 dehydro-beta-ionone 5,6-环氧化物 6-epoxide
910.053-oxo- dihydro-alpha-紫罗兰 ionol
450.01  二氢-α-紫罗兰酮 dihydro-alpha-ionone
870.103-oxo- 二氢-α-紫罗兰酮 dihydro-alpha-ionone
820.20(E+Z)-二氢-α-紫罗兰酮 dihydro-alpha-ionone 肟 oxime
600.40  二氢β-紫罗兰醇 dihydro-beta-ionol
930.203-oxo- 二氢β-紫罗兰醇 dihydro-beta-ionol
1290.01 二氢β-紫罗兰醇 dihydro-beta-ionol 5,6-环氧化物 6-epoxide
460.30  二氢β-紫罗兰酮 dihydro-beta-ionone
1570.054-oxo-二氢β-紫罗兰酮 dihydro-beta-ionone
830.40(E+Z)-二氢β-紫罗兰酮 dihydro-beta-ionone 肟 oxime
500.02 dihydro-beta-ionyl 甲 formate
1710.03  二氢actinidiolide dihydroactinidiolide
740.02  二氢博伏利特 bovolide
610.037-oxo-dihydrotheaspirane a1
670.037-oxo-dihydrotheaspirane a2
620.027-oxo-dihydrotheaspirane b1
680.027-oxo-dihydrotheaspirane b2
1670.022,3-dimethyl-2-nonen-4-olide
120trace(E)-6,10- dimethyl-5,9-undecadien-2-ol 9-undecadien-2-ol
130trace5,8-epidi氧 oxy-6-megastigmen-9-ol
153trace2,3- epoxy-2,6,6-三甲基环己-1 6-trimethyl cyclohexan-1,4-二酮 4-dione
1840.01  2-羟基-3-甲基戊酸乙酯 ethyl 2-hydroxy-3-methyl valerate
178trace  2-甲基丁酸乙酯 ethyl 2-methyl butyrate
179trace  3-甲基丁酸乙酯 ethyl 3-methyl butyrate
220.50  苯甲酸乙酯 ethyl benzoate
1770.01  丁酸乙酯 ethyl butyrate
181trace  己酸乙酯 ethyl caproate
196trace  辛酸乙酯 ethyl caprylate
233trace  肉桂酸乙酯 ethyl cinnamate
2380.03  ethyl nicotinate
183trace  钛酸乙酯 ethyl tiglate
690.30  eugenol
770.10异 iso eugenol
430.80(E,E)-alpha- farnesene
1250.20(E,E)- 法尼醇 farnesol
1380.01  geranial
1580.10  geranic acid
1240.02  香叶醇 geraniol
207trace  乙酸香叶酯 geranyl acetate
480.04(E)- 香叶基丙酮 geranyl acetone
206trace  香叶酸香叶酯 geranyl formate
1270.30  香叶基芳樟醇 geranyl linalool
1030.10  germacrene D
1490.012- heptadecanone
1070.01  heptanol
252trace  庚腈 heptanonitrile
255trace  十六烷酰基 hexadecanonitrile
90.02  hexanol
106trace(E)-2- hexenal
100.01(z)-3 Z)-3- 己烯-1-醇 hexen-1-ol
70.01(z)-3 Z)-3- 己烯-1-基乙酸酯 hexen-1-yl acetate
192trace(z)-3 Z)-3- 己烯-1-基乙酸酯 hexen-1-yl acetate
1910.05(z)-3 Z)-3- hexen-1-yl benzoate
189trace(z)-3 Z)-3- hexen-1-yl butyrate
188trace(z)-3 Z)-3- hexen-1-yl 甲 formate
1900.02(z)-3 Z)-3- hexen-1-yl tiglate
186trace  乙酸己酯 hexyl acetate
1870.05  苯hexyl benzoate
185trace  hexyl formate
102tracealpha- humulene
136tracepara- 羟基茴香醚 hydroxyanisole
784.00  吲哚 indole
550.03(E)-beta- 紫罗兰 ionol
1560.054-oxo-beta- 紫罗兰 ionol
510.10alpha- 紫罗兰 ionol
128tracebeta- 紫罗兰 ionol 5,6-环氧化物 6-epoxide
470.03(E)-alpha- ionone
540.20(E)-beta- ionone
560.10beta-ionone 5,7-epoxide
860.50(E)-alpha-ionone 肟 oxime
890.90(E)-beta-ionone 肟 oxime
850.20(Z)-alpha-ionone 肟 oxime
880.30(Z)-beta-ionone 肟 oxime
208tracebeta-ionyl 甲 formate
490.05(Z)- jasmone
2490.02 jasmone 肟 oxime
3trace  柠檬烯 limonene
160.80  linalool
120.20(Z)- linalool oxide furanoid
350.20(E)- linalool oxide pyranoid
312.50(Z)- linalool oxide pyranoid
1631.00  linoleic acid
1640.50  亚麻酸 linolenic acid
193trace  (e)-2-己酸甲酯 methyl (E)-2-hexenoate
260.02 methyl (E)-3-methyl-4-decenoate
800.14 methyl (E)-茉莉 jasmonate
194trace  (z)-3-己酸甲酯 methyl (Z)-3-hexenoate
2010.01 methyl (z)-3 Z)-3-methyl-4-decenoate
2000.02  (z)-4-癸烯酸甲酯 methyl (Z)-4-decenoate
790.06  (z)-茉莉酸甲酯 methyl (Z)-jasmonate
110.01  methyl 2-hydroxy-3-丁酸甲酯 methyl butyrate
130.02 m2-羟基-3-甲基戊酸乙酯 ethyl 2-hydroxy-3-methyl valerate
1750.01  2-丁酸甲酯 methyl 2-methyl butyrate
1760.01  m3-甲基丁酸乙酯 ethyl 3-methyl butyrate
2340.02  methyl 5-苯基 -phenyl valerate
239trace4- methyl anisole
729.00  邻氨基苯甲酸甲酯 methyl anthranilate
175.00  苯甲酸甲酯 methyl benzoate
1040.012- methyl butanol
105trace3- methyl butanol
140.02(E+Z)-2- methyl 丁醛肟 butyrald肟 oxime
150.02(E+z)-3 Z)-3- methyl 丁醛肟 butyrald肟 oxime
174trace  丁酸甲酯 methyl butyrate
1trace2- methyl 丁腈 butyronitrile
199trace  癸酸甲酯 methyl caprinate
180trace  己酸甲酯 methyl caproate
1950.02  辛酸甲酯 methyl octanoate
2320.05  肉桂酸甲酯 methyl cinnamate
2420.10  甲基丁香酚 methyl eugenol
2040.05  香叶酸甲酯 methyl geranate
173trace  异丁酸甲酯 methyl isobutyrate
2430.20  甲基异丁香酚 methyl isoeugenol
2500.02(Z)-methyl 茉莉 jasmonate 肟 oxime
2020.15  月桂酸甲酯 methyl laurate
942.01  亚油酸甲酯 methyl linolenate
960.50  亚油酸甲酯 methyl linolenate
2360.10  正乙酰邻氨基苯甲酸甲酯 methyl N-acetyl anthranilate
650.02  methyl 正乙基 N-ethyl 邻氨基苯甲酸 anthranilate
2370.10  methyl 正甲酰基 N-formyl 邻氨基苯甲酸 anthranilate
630.05  正甲基邻氨基苯甲酸甲酯 methyl N-methyl anthranilate
280.15  烟酸甲酯 methyl nicotinate
810.20  棕榈酸甲酯 methyl palmitate
320.10  乙酸甲基苯酯 methyl phenyl acetate
340.15  水杨酸甲酯 methyl salicylate
920.20  硬脂酸甲酯 methyl stearate
182trace  替格酸甲酯 methyl tiglate
2350.01  香草酸甲酯 methyl vanillate
5trace2- methyl-1-nitrobutane
146trace(E)-3- methyl-2-nonen-4-one
1190.02(E)-3- methyl-4-decen-1-ol
410.02(E)-3- methyl-4-decen-1-ol
580.043- methyl-5-(2,6,6-三甲基环己-1-烯-1-基)异恶唑 6-trimethyl cyclohex-1-en-1-yl) isoxazole
80.026- 甲基-5-庚-2-酮 methyl-5-hepten-2-one
440.03(E+Z)-6- 甲基-5-庚-2-酮 methyl-5-hepten-2-one 肟 oxime
99trace  myrcene
137trace  neral
1230.01  橙花醇 nerol
700.40(E)- 橙花醇 nerolidol
205trace  甲酸橙花酯 neryl formate
590.101- nitro-2-phenethane
165trace  nonan-4-olide
1140.03  nonanol
1450.022- nonanone
2470.012- nonanone 肟 oxime
1170.02(Z,z)-3 Z)-3,6- nonen-1-ol
115trace(z)-3 Z)-3- nonen-1-ol
116trace(Z)-6- nonen-1-ol
1980.01(Z)-6- nonen-1-yl acetate
166trace2- nonen-4-olide
60.20(E)-beta- 罗勒烯 ocimene
1000.02(Z)-beta- 罗勒烯 ocimene
113trace(E,e)-2 E)-2,4- octadien-1-ol
1120.01(Z,Z)-2,5-octadien-1-ol
1080.05  辛基酚聚醚 octanol
1440.013- octanone
246trace3- octanone 肟 oxime
253trace  辛腈 octanonitrile
110trace(E)-2- octen-1-ol
109trace(Z)-2- octen-1-ol
1110.01(Z)-5- octen-1-ol
1970.05(Z)-5- octen-1-yl acetate
1610.20  棕榈酸 palmitic acid
1480.012- pentadecanone
390.302- 醋酸苯乙酯 phenethyl acetate
4230.002- 苯乙醇 phenethyl alcohol
950.502- 苯甲酸苯乙酯 phenethyl benzoate
2200.012- phenethyl butyrate
2230.052- phen己酸乙酯 ethyl caproate
2240.052- 辛酸苯乙酯 phenethyl caprylate
330.302- 甲酸苯乙酯 phenethyl formate
219trace2- 异phenethyl isobutyrate
2210.022- 异戊酸苯乙酯 phenethyl isovalerate
241trace2- 苯乙基 phenethyl methyl ether
2250.202- 苯乙乙酸苯酯 phenethyl phenyl acetate
2220.022- 钛酸苯乙酯 phenethyl tiglate
132trace  phenol
1410.02  苯乙醛 phenyl acetaldehyde
761.00(E+Z)- phenyl 乙醛肟 acetald肟 oxime
230.01(E+Z)-phenyl 乙醛肟 acetald肟 oxime-O-methyl ether
1600.20  苯乙酸 phenyl acetic acid
142trace  苯phenyl propionaldehyde
2270.053- 乙酸苯丙酯 phenyl propyl acetate
1310.023- 苯phenyl propyl alcohol
2260.053- phenyl propyl 甲 formate
1260.30  植醇 phytol
97tracealpha- 松油萜、蒎烯 pinene
20.01beta- 松油萜、蒎烯 pinene
98trace  桧烯 sabinene
245trace  safrole
1620.50  硬脂酸 stearic acid
1210.03  terpinen-4-ol
270.10alpha- 松油醇 terpineol
254trace  四癸腈 tetradecanonitrile
840.054,4a 4a,5,6-tetrahydro-4,4,7-trimethyl-2(3h H)-萘酮 -naphthalenone
190.021,2,5,5-tetramethyl octahydroquinoline
660.031,3,7,7-tetramethyl-2-oxabicyclo(4.4.0)decan-9-one
290.202,5,5,8a- tetramethyl-6,7,8,8a-tetrahydro-1(5h H)-1-benzopyran
180.02  theaspirane A
200.02  theaspirane A
1470.022- 十三烷酮 tridecanone
1520.012,6,6- trimethyl cyclohexan-1,4-二酮 4-dione
1500.206,10,14- trimethyl pentadecan-2-one
2480.056,10,14-trimethyl pentadecan-2-one 肟 oxime
1510.052,6,6- trimethyl-2-cyclohexen-1,4-二酮 4-dione
300.012,5,5-trimethyl-5,6,7,8-tetrahydroquinoline
240.012- 十一烷酮 undecanone
135tracepara- vinyl phenol

R. 石莲子/云实 k Kaiser, New 易挥发的 volatile 成分 constituents of the 花 flower 浸膏 concrete of 米契里亚 Michelia champaca champaca L. In: Proceedings of 11th International Congress of 必要 Essential 油类 Oils, 香精 Fragrances 风味 Flavours. Edits., S. C. Bhattacharyya, N. Sen K. L. Sethi, p. 1-13, 牛津 Oxford &amp & ibh i IBh H 出版 Publishing Co., pvt Pvt. ltd Ltd, New delhi Delhi (1989).

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